HAPPI - January 2014

Formulary

Product formulas are supplied by producers of raw materials.

Included in some instances are sources of supply for the raw materials and instructions for preparation and use of the finished product. No guarantee of performance or safety is implied by Happi.

For more complete details, readers should contact the suppliers directly using the telephone number or website provided with each formula. If your company has a formula that you think would be of interest to readers of Happi, marketers of soaps and detergents;

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disinfectants and sanitizers and other chemical specialties, we will be pleased to consider it for publication. Address all material to: Formulary Editor, Happi, 70 Hilltop Rd., Ramsey, NJ 07446 USA;

Email: tbranna@rodmanmedia.com

AkzoNobel Surface Chemistry Personal Care
888-331-6212 • Fax: 908-707-3664
Email: personalcare.usa@akzonobel.com
www.akzonobel.com/PersonalCare

INGREDIENTS W T%

Phase A

Deionized water 76. 77

Dissolvine NA2-S chelate (AkzoNobel 0.10

Functional Chemicals) (Disodium EDTA)

Flexan II polymer (AkzoNobel Personal Care) 3.00

(Sodium polystyrene sulfonate)

Propylene glycol (Sinopharm Chemical) 3.00

Structure XL starch (AkzoNobel Personal Care) 1.00

(Hydroxypropyl starch phosphate)

Carbopol 940 (Lubrizol) 0.40

Phase B

Montanov 68 (Seppic )(Cetearyl alcohol (and) 1.50 cetearyl glucoside)

Arlacel 165 (Croda, Inc.) (Glyceryl stearate (and) 1.00

PEG-100 stearate)

Lanette O (BASF) (Cetearyl alcohol) 2.00 Cetiol SB 45 (BASF) (Butyrospermum 1.00 parkii (shea butter))

Cetiol CC (BASF) (Dicaprylyl carbonate) 3. 50

Xiameter PMX-200 Silicone Fluid 100 cs 1.00

(Dow Corning) (Dimethicone)

Phase C

Triethanolamine-99% (Dow Chemical) 0.40 Hydrovance moisturizing agent (50% solids) 2.00 (AkzoNobel Personal Care) (Hydroxyethyl urea)

Citroflex 2 (Vertellus Performance Materials Inc.) 0.18 (Triethyl citrate)

Citric acid (Sinopharm Chemical) 0.01 Tri-Sodium citrate dihydrate (Sinopharm Chemical) 0.04 Phase D

Dry-Flo TS starch (AkzoNobel Personal Care) 2.00 (Tapioca starch (and) polymethylsilsesquioxane)

Dry-Flo Pure starch (AkzoNobel Personal Care) 1.00 (Aluminum starch octenylsuccinate)

Phase E

Euxyl K220 (schülke & mayr) (Methylisothiazolinone 0.10 (and) ethylhexylglycerin (and) water)

PROCEDURE: To the main vessel, add deionized water, Dissolvine NA2-S chelate and propylene glycol. Mix until dissolved using a propeller with moderate speed. Sprinkle in Carbopol 940, and mix until dispersed. Then add Flexan II polymer and Structure XL starch, one at a time. Ensure that the polymers are hydrated and homogeneously dispersed. Begin to heat phase A to 75-80°C. Combine phase B in a side kettle and mix with a propeller at moderate speed, heating to 75-80°C. Slowly add phase B into phase A under a homogenizer with moderate speed. Emulsify for 1 minute. Switch the batch to propeller, and begin cooling the batch to 65°C while mixing. Neutralize the batch with triethanolamine. Mix moderately for 10 minutes until uniform. Add the remaining ingredients from phase C, and mix until homogeneous. Continue to cool the batch to 45°C. Add phase D at low speed under the homogenizer. Move the beaker around to allow full incorporation of the starches, approximately 10 minutes. Add phase E, and mix until homogeneous. Switch the batch to a sweep blade, and cool to room temperature. Drop the batch. PROPERTIES: pH— 6-7; Viscosity—18000-30000 cps (Brookfield viscometer RVDV-II+, RV 6#, 10 rpm, 25 ºC); Appearance—White Cream; Color—White; Packaging—Dual-tube bottle.